一、電子煙釋放物技術要求
1.氣溶膠釋放穩(wěn)定性
|
Test Items |
Limit 限值 |
Test Method |
|
氣溶膠釋放穩(wěn)定性 |
氣溶膠捕集的每個檢測結果與平均值的相對偏差不超過25% |
附錄C |
電子煙抽煙機
1）氣溶膠捕集量的測定條件：
電子煙吸煙機條件（抽吸時間：3±0.1s,抽吸頻率：30±0.5s，抽吸容量55±0.3mL）
測試電子煙樣品數(shù)量為3支（準備樣品至少抽吸數(shù)量的3倍）
口數(shù)大于100口：每抽吸20口捕集到同一張濾片上，依次抽吸5次，取第1，3，5張濾片進行分析;
口數(shù)大于60口：每抽吸20口捕集到同一張濾片上，依次抽吸3次，分別對張濾片進行分析;
口數(shù)小于60口：每抽吸10口捕集到同一張濾片上，依次抽吸3次，分別對張濾片進行分析;
2.煙堿釋放穩(wěn)定性
|
Test Items |
Limit 限值 |
Test Method |
|
煙堿釋放穩(wěn)定性 |
煙堿釋放量每個檢測結果與平均值的相對偏差不超過25% |
附錄I |
氣相色譜儀
3.羰基化合物限量
|
Category |
Test Items |
Limit |
Test Method |
|
Carbonyl Compounds |
Formaldehyde |
200 |
附錄J |
|
Acetaldehyde |
3200 |
||
|
Acrolein |
16 |
||
|
Diacetyl(2，3-Butadione) |
140 |
4.重金屬限量
|
Category |
Test Items |
Limit |
Test Method |
|
Heavy Metals |
Cd(Cadmium)鎘 |
0.2 |
GB5009.268 |
|
Cr(Chromium)鉻 |
0.3 |
||
|
Pb(Lead)鉛 |
0.5 |
||
|
Ni(Nickel)鎳 |
0.5 |
||
|
Sb(Antimony)銻 |
2 |
||
|
As(Arsenic)砷 |
0.2 |
||
|
Hg(Mercury)汞 |
0.1 |
電感耦合等離子體質(zhì)譜儀
對比化學測試項目(GB&FDA&TPD)
|
Type |
Category |
Test Items |
GB |
FDA |
TPD |
Remark |
|
煙油類 |
Nicotine Consistency |
Anabasine |
X |
√ |
X |
FDA定義了安納巴松 |
|
Nicotine(a power level,5 data of nicotine) |
√ |
√ |
√ |
|||
|
Carbonyl Compounds |
Formaldehyde |
20 |
√ |
√ |
|
|
|
Acetaldehyde |
20 |
√ |
√ |
|||
|
Acrolein |
16 |
√ |
√ |
|||
|
Crotonaldehyde |
X |
√ |
√ |
|||
|
Diacetyl(2，3-Butadione) |
20 |
√ |
√ |
|||
|
Acetyl Propionyl |
X |
√ |
X |
|||
|
Pentane 2,3 dione |
X |
X |
√ |
|||
|
Heavy Metals |
Cd(Cadmium) |
0.2 |
√ |
√ |
GB管控6種 |
|
|
Cr(Chromium) |
0.3 |
√ |
√ |
|||
|
Pb(Lead) |
0.5 |
√ |
√ |
|||
|
Ni(Nickel) |
0.5 |
√ |
√ |
|||
|
Sb(Antimony) |
X |
X |
√ |
|||
|
As(Arsenic) |
0.2 |
X |
√ |
|||
|
Fe(Iron) |
X |
X |
√ |
|||
|
Al(Aluminum) |
X |
X |
√ |
|||
|
Sn(Tin) |
X |
X |
√ |
|||
|
Hg(Mercury) |
0.1 |
X |
√ |
|||
|
Cu(Copper) |
X |
X |
√ |
|
Type |
Category |
Test Items |
GB |
FDA |
TPD |
Remark |
|
煙油類 |
Ammonia |
Ammonia |
X |
√ |
X |
FDA |
|
Aromatic Amines |
4-Aminobiphenyl |
X |
√ |
X |
FDA |
|
|
1-Aminonaphthalene |
X |
√ |
X |
|||
|
2-minonaphthalene |
X |
√ |
X |
|||
|
Polyartomatic Hydrocarbon |
Benzo(a)pyrene |
X |
√ |
X |
FDA |
|
|
Glycol |
Menthol |
X |
√ |
X |
FDA提到薄荷醇 |
|
|
Methanol |
√ |
X |
X |
|||
|
Ethylene Glycol |
√ |
√ |
√ |
|||
|
Diethylene Glycol |
√ |
√ |
√ |
|||
|
Tobacco-Specific Nittrosamines |
4-(N-methylnitrosamino)-1-(3-pyridyl)-1-butanone(NNK) |
√ |
√ |
√ |
GB提到NAB+NAT |
|
|
N-nitrosonornicotine(NNN) |
√ |
√ |
√ |
|||
|
N-亞硝基假本賊堿(NAB) |
√ |
X |
X |
|||
|
N-亞硝基新煙堿 |
√ |
X |
X |
|||
|
Volatile |
Acrylonitrile |
X |
√ |
X |
FDA提到丙烯腈 |
|
|
Benzene |
√ |
√ |
√ |
|||
|
1,3-Butadiene |
X |
√ |
√ |
|||
|
Isoprene |
X |
√ |
√ |
|||
|
Toluene |
√ |
√ |
√ |
|||
|
乙苯 |
√ |
X |
X |
|||
|
二甲苯(含對二甲苯,間二甲苯鄰二甲苯) |
√ |
X |
X |
|||
|
鄰苯二甲酸酯類 |
17種鄰苯二甲酸酯類物質(zhì)總量 |
√ |
X |
X |
GB |
|
Type |
Category |
Test Items |
GB |
FDA |
TPD |
Remark |
|
釋放物類 |
氣溶膠釋放穩(wěn)定性 |
氣溶膠釋放穩(wěn)定性 |
25% |
X |
X |
GB |
|
煙堿釋放穩(wěn)定性 |
Nicotine |
25% |
√ |
√ |
GB提到偏差量 |
|
|
Carbonyl Compounds |
Formaldehyde |
200 |
X |
200 |
GB管控4項 |
|
|
Acetaldehyde |
3200 |
X |
3200 |
|||
|
Acrolein |
16 |
X |
16 |
|||
|
Crotonaldehyde |
X |
X |
√ |
|||
|
Diacetyl(2，3-Butadione) |
140 |
X |
X |
|||
|
Heavy Metals |
Cd(Cadmium) |
0.2 |
√ |
2 |
GB管控7項 |
|
|
Cr(Chromium) |
0.3 |
√ |
3 |
|||
|
Pb(Lead) |
0.5 |
√ |
5 |
|||
|
Ni(Nickel) |
0.5 |
√ |
5 |
|||
|
Sb(Antimony) |
2 |
X |
20 |
|||
|
As(Arsenic) |
0.2 |
X |
√ |
|||
|
Fe(Iron) |
X |
X |
√ |
|||
|
Al(Aluminum) |
X |
X |
√ |
|||
|
Sn(Tin) |
X |
X |
√ |
|||
|
Hg(Mercury) |
0.1 |
X |
√ |
|||
|
Cu(Copper) |
X |
X |
√ |
|||
|
Ammonia |
Ammonia |
X |
√ |
X |
FDA |
|
|
Humectants |
Ethylene Glycol |
X |
√ |
X |
FDA |
|
|
Diethylene Glycol |
X |
√ |
X |
|||
|
Glycerol |
X |
√ |
X |
|||
|
Propylene Glycol |
X |
√ |
X |
|||
|
Nitrosamines,TSNA |
NNK |
X |
√ |
X |
FDA |
|
|
NNN |
X |
√ |
X |
